International Journal of Nano Dimension (Int. J. Nano Dimens.) Synthesis and characterization of Silver-Silica heterogeneous nanocomposite particles by Lithium Aluminum Hydroxide reducing method Volume 3 (2012) Issue 4, June 2013 2024 03 01 Synthesis and characterization of Silver-Silica heterogeneous nanocomposite particles by Lithium Aluminum Hydroxide reducing method 10.7508/ijnd.2012.04.003 EN Babak Sadeghi Department of Chemistry, Islamic Azad University, Tonekabon Branch, Tonekabon, IRAN. 0000-0003-0933-5782 Sh. Ghammamy Department of Chemistry, Faculty of Science, Imam Khomeini International University, Qazvin, Iran. S. Sedaghat Department of Chemistry, Shahr-e-Qods Branch, Islamic Azad University, Tehran, Iran Journal Article 2024 03 01 We have used Lithium Aluminum Hydroxide reducing method of silver nitrate to prepare heterogeneous silver-silica nanocomposite particles with thiol and amino groups serving to bind the Ag nanoparticles to the surfaces of the SiO2 nanoparticles. We examined products of these reductions using FTIR, SEM, XRD and UV-vis. spectroscopy. The SiO2 nanoparticles had diameters ranging from 70 to 90 nm; the Ag nanoparticles that formed on the surfaces of the SiO2 nanoparticles had an average size of ca. 15 nm.